A new compact symmetric rotational diamond anvil cell for in situ high-pressure-torsion studies

In situ studies under severe plastic deformation at high pressures, employing rotational/shear diamond anvil cells (RDAC), have recently gained much interest in the high-pressure community owing to their potential applications in material processing methods, mechanochemistry, geophysics, etc. These studies, combined with multi-scale computational simulations, provide important insights into the transient hierarchical microstructural evolution, structural phase transitions, and orientation relationship between parent and daughter phases and help establish the kinetics of strain-induced phase transitions under severe plastic deformation. Existing RDACs are mostly used in axial x-ray diffraction geometry due to geometrical constraints providing less reliable information about stress states and texture. Their asymmetric design also poses serious limitations to high-pressure shear studies on single crystals. To overcome these limitations, a new compact symmetric rotational diamond anvil cell has been designed and developed for in situ high-pressure torsion studies on materials. The symmetric angular opening and short working distance in this new design help obtain a more reliable crystallographic orientation distribution function and lattice strain states up to a large Q range. Here, we present the advantages of the symmetric design with a few demonstrative studies.

K. K. Pandey, H. K. Poswal · 2023